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Yes, I have attempted to Immunize again, but was not successful.

To answer your questions:

Which items are not immunized exactly?
Default (cookies)
Default (images)
Default (installations)
Default (Popups)

Did you closed the browser while immunizing?...

Thanks for the info. However, when I attempt immunization, Firefox 3 (my default) remains unprotected. I am using Spybot 1.6.

Am I doing something wrong?

Does Spybot-S&D recognize/enable immunization for Firefox 3.0 and Google Chrome?

Thanks!